东昆仑五龙沟地区晚志留世A型花岗岩成因:U-Pb年代学、地球化学、Nd及Hf同位素制约

王艺龙; 李艳军; 魏俊浩; 李欢; 韩玉; 周红智; 黄啸坤; 柯坤家

doi:10.3799/dqkx.2018.717

东昆仑五龙沟地区晚志留世A型花岗岩成因:U-Pb年代学、地球化学、Nd及Hf同位素制约

doi: 10.3799/dqkx.2018.717

王艺龙^1,2,,
李艳军^1,3, ,,
魏俊浩^1,3,
李欢¹,
韩玉⁴,
周红智¹,
黄啸坤¹,
柯坤家¹

1.
中国地质大学资源学院, 湖北武汉 430074
2.
辽宁省地质勘查院, 辽宁大连 116100
3.
固体矿产勘查国家级实验教学示范中心, 湖北武汉 430074
4.
青海省第一地质矿产勘查院, 青海平安 810600

基金项目:

国家自然科学基金项目 41672083

国家自然科学基金项目 41202054

中央高校基本科研业务费区域引导专项 CUGQYZX1708

中国地质调查局地质调查项目 12120114081101

详细信息

作者简介:
王艺龙(1990-), 男, 工程师, 主要从事区域地质调查工作

通讯作者:
李艳军, E-mail:liyanjun21023@163.com

中图分类号: P597
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- 被引次数: 0
出版历程
- 收稿日期: 2017-12-20
- 刊出日期: 2018-04-15

Origin of Late Silurian A-Type Granite in Wulonggou Area, East Kunlun Orogen: Zircon U-Pb Age, Geochemistry, Nd and Hf Isotopic Constraints

Wang Yilong^{1,2
,},
Li Yanjun^{1,3
, ,},
Wei Junhao^1,3,
Li Huan¹,
Han Yu⁴,
Zhou Hongzhi¹,
Huang Xiaokun¹,
Ke Kunjia¹

1.
Faculty of Earth Resources, China University of Geosciences, Wuhan 430074, China
2.
Geological Exploration Institute of Liaoning Province, Dalian 116100, China
3.
National Demonstration Center for Experimental Mineral Exploration Education, Wuhan 430074, China
4.
Qinghai No.1 Academy of Geology and Mineral Exploration, Ping'an 810600, China

摘要

摘要: 东昆仑造山带东段五龙沟金矿田内首次发现晚志留世A型花岗岩体.对其开展了锆石U-Pb年代学、岩石地球化学、Nd及Hf同位素研究，探讨岩体成因和构造背景.岩体LA-ICP-MS锆石U-Pb定年结果为420±3 Ma，为晚志留世岩浆活动产物.岩石具有高SiO₂（76.0%~78.4%）、K₂O（4.64%~5.22%）和Na₂O（2.93%~3.25%）含量，低FeO^T（0.98%~1.45%）、MgO（0.11%~0.22%）和CaO（0.27%~0.79%）含量特征.样品富集大离子亲石元素（Rb、K、La）和LREE，亏损高场强元素（Nb、P、Ti）和HREE，具有强烈的Eu负异常（Eu/Eu^*=0.09~0.12）.该岩体10⁴×Ga/Al比值为3.09~3.15，具有A型花岗岩的特征.全岩ε_Nd（t）=-2.5~-2.2，对应的二阶段模式年龄t_DM2（Nd）=1 339~1 365 Ma.锆石ε_Hf（t）=-2.8~+2.1，二阶段模式年龄t_DM2（Hf）=1 269~1 583 Ma.地球化学、Nd及Hf同位素揭示该岩体为软流圈地幔部分熔融形成的幔源岩浆与其诱发的古老地壳物质混合形成.构造判别图解指示岩体具有A₂型花岗岩特征，形成于后碰撞伸展构造环境.结合和勒冈那仁和冰沟A型花岗岩体，认为东昆仑地区至少在晚志留世已进入伸展阶段.
- A型花岗岩 /
- 晚志留世 /
- 岩石成因 /
- 后碰撞伸展 /
- 东昆仑 /
- 岩石学 /
- 地球化学
Abstract: Late Silurian A-type granite is reported for the first time in the Wulonggou gold district, eastern segment of the Kunlun orogenic belt. This paper presents (1) laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) U-Pb age for the Wulonggou A-type granite to determine precisely the time of the magmatism, (2) geochemical, Nd and Hf isotope data for the Wulonggou A-type granite to constrain the petrogenesis and tectonic setting. The LA-ICP-MS U-Pb analyses of zircon from the Wulonggou A-type granite yielded a weighted mean ²⁰⁶Pb/²³⁸U age of 420±3 Ma, indicating that it was emplaced in the Late Silurian. All rock samples are enriched in SiO₂ (76.0%-78.4%), K₂O (4.64%-5.22%) and Na₂O (2.93%-3.25%), but with relatively low concentrations of FeO^T (0.98%-1.45%), MgO (0.11%-0.22%) and CaO (0.27%-0.79%). Samples are also enriched in large ion lithophile elements (Rb, K, La) and light rare earth elements, but depleted in high field strength elements (Nb, P, Ti) and heavy rare earth elements with strong negative Eu anomalies (Eu/Eu^*=0.09-0.12). The 10⁴×Ga/Al ratios of the Wulonggou A-type granites vary from 3.09 to 3.15. Mineralogy and geochemistry of the rocks show an affinity with aluminous A-type granite. The ε_Nd(t) values of whole-rock range from -2.5 to -2.2 with corresponding two-stage Nd model ages ranging from 1 339 to 1 365 Ma. The ε_Hf(t) values of zircon vary from -2.8 to +2.1 and two-stage Hf model ages range from 1 269 to 1 583 Ma. The Nd and Hf isotopic data imply that different source materials have contributed to the magma genesis. Integrated geological, geochemical and isotopic data suggest that Wulonggou A-type granite is most likely generated via the mixture of asthenosphere-derived magma and the ancient crustal materials. The A-type granite was marked by A₂ type and was formed in post-collisional extensional tectonic environment. In combination with the A-type granites such as those in the Helegangnaren and Binggou, it is concluded that the eastern Kunlun area had begun its post-orogenic extension stage since Late Silurian, and this stage continued at least about 34 Ma.
- A-type granite /
- Late Silurian /
- petrogenesis /
- post-collisional extensional setting /
- East Kunlun orogen /
- petrology /
- geochemistry

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图 1 东昆仑构造位置图(a)，东昆仑地区地质简图(b)和红旗沟岩体地质简图(c)

图a据Xu et al.(2001)；图b修编自Zhang et al.(2014)

Fig. 1. Geotectonic framework (a), geological map of the East Kunlun orogen belt (b) and simplified geological map of the Hongqigou granite (c)

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图 2 五龙沟地区红旗沟正长花岗岩野外照片(a)和镜下照片(正交偏光)(b)

Kfs.碱性长石；Pl.斜长石；Bi.黑云母；Q.石英

Fig. 2. Field pictures (a) and microphotographs (b) of the Hongqigou syenogranite from the Wulonggou area

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图 3 红旗沟正长花岗岩样品(WSMG-1)典型锆石CL图及U-Pb定年结果

实线圈和虚线圈分别代表U-Pb和Hf同位素分析测试点

Fig. 3. Cathodoluminescence images for zircons of sample WSMG-1 showing sites of U-Pb (solid circles) and Hf (dashed circles) analyses

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图 4 红旗沟正长花岗岩K₂O-SiO₂(a)和A/NK-A/CNK(b)关系

图a底图据Collins et al.(1982)；图b底图据Maniar and Piccoli(1989).数据来源：和勒冈那仁碱长花岗岩据Li et al.(2013)；冰沟正长花岗岩据刘彬等(2013a)

Fig. 4. K₂O vs. SiO₂ (a) and A/NK vs. A/CNK (b) diagrams for the Hongqigou syenogranite

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图 5 红旗沟正长花岗岩稀土元素球粒陨石标准化配分图(a)和微量元素原始地幔标准化蛛网图(b)

标准化数据引自Sun and McDonough(1989).数据来源同图 4

Fig. 5. Chondrite-normalized REE patterns (a) and primitive mantle-normalized trace element patterns (b) for the Hongqigou syenogranite

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图 6 红旗沟正长花岗岩成因类型判别图解

底图据Whalen et al.(1987)；数据来源同图 4

Fig. 6. Petrogenesis discrimination diagrams for the Hongqigou syenogranite

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图 7 红旗沟正长花岗岩锆石Hf同位素组成图解(a)和t-ε_Nd(t)图解(b)

数据来源：东昆仑基底据余能等(2005)；胡晓钦镁铁质岩石据刘彬等(2013b)；Yikehalaer花岗闪长岩据Li et al.(2015)；猴头沟二长花岗岩据严威等(2016)；跃进山辉长岩据刘彬等(2012)；冰沟正长花岗岩据刘彬等(2013a)；红旗沟辉长岩为项目组未发表数据

Fig. 7. Hf isotopic compositions of zircons (a) and t-ε_Nd(t) (b) diagrams for the Hongqigou syenogranite

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图 8 红旗沟正长花岗岩Rb-(Y+Nb)(a)和Rb/30-Hf-Y-3Ta(b)构造环境判别图解

图a底图据Pearce(1996)；图b底图据Harris et al.(1986)数据来源同图 4

Fig. 8. Rb vs. Y+Nb (a) and Rb/30-Hf-Y-3Ta (b) discrimination diagrams of the Hongqigou syenogranite

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图 9 红旗沟正长花岗岩R₁-10⁴×Ga/Al(a)和Nb-Y-3Ga(b)图解

图a据Hong et al.(1996)；图b据Eby(1992).数据来源同图 4

Fig. 9. R₁ vs. 10⁴×Ga/Al (a) and Nb-Y-3Ga (b) diagrams of the Hongqigou syenogranite

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表 1 五龙沟地区红旗沟正长花岗岩(WSMG-1)锆石LA-ICP-MS U-Pb定年分析数据

Table 1. Zircon LA-ICP-MS U-Pb data of the Hongqigou syenogranite sample (WSMG-1) from Wulonggou area

点号	²³²Th (10^-6)	²³⁸U (10^-6)	Th/U	U-Th-Pb同位素比值								年龄(Ma)
点号	²³²Th (10^-6)	²³⁸U (10^-6)	Th/U	²⁰⁷Pb/²⁰⁶Pb	1σ	²⁰⁷Pb/²³⁵U	1σ	²⁰⁶Pb/²³⁸U	1σ	²⁰⁸Pb/²³²Th	1σ	²⁰⁷Pb/²⁰⁶Pb	1σ	²⁰⁷Pb/²³⁵U	1σ	²⁰⁶Pb/²³⁸U	1σ	²⁰⁸Pb/²³²Th	1σ
WSMG-1-01	399	652	0.61	0.05570	0.00135	0.51460	0.01491	0.06701	0.00089	0.02246	0.00077	440	53	422	10	418	5	449	15
WSMG-1-02	290	317	0.92	0.05530	0.00150	0.51297	0.01615	0.06728	0.00093	0.02009	0.00070	424	59	420	11	420	6	402	14
WSMG-1-03	130	172	0.75	0.05586	0.00156	0.52080	0.01744	0.06763	0.00099	0.01950	0.00059	447	61	426	12	422	6	390	12
WSMG-1-04	231	330	0.70	0.05585	0.00141	0.51808	0.01536	0.06728	0.00090	0.02067	0.00069	446	55	424	10	420	5	414	14
WSMG-1-05	446	605	0.74	0.05529	0.00164	0.50959	0.01696	0.06685	0.00093	0.02315	0.00127	424	64	418	11	417	6	463	25
WSMG-1-06	273	399	0.68	0.05532	0.00123	0.51679	0.01438	0.06776	0.00091	0.02038	0.00050	425	48	423	10	423	5	408	10
WSMG-1-07	173	351	0.49	0.05558	0.00190	0.51689	0.01950	0.06748	0.00100	0.02060	0.00122	435	74	423	13	421	6	412	24
WSMG-1-08	227	234	0.97	0.05546	0.00232	0.51464	0.02357	0.06732	0.00112	0.01983	0.00123	431	91	422	16	420	7	397	24
WSMG-1-09	167	252	0.66	0.05542	0.00192	0.51702	0.01964	0.06764	0.00101	0.02066	0.00120	429	75	423	13	422	6	413	24
WSMG-1-10	460	660	0.70	0.05584	0.00141	0.51730	0.01552	0.06718	0.00092	0.02320	0.00102	446	55	423	10	419	6	464	20
WSMG-1-11	143	148	0.97	0.05558	0.00242	0.51522	0.02438	0.06723	0.00113	0.01984	0.00120	436	94	422	16	420	7	397	24
WSMG-1-12	225	288	0.78	0.05536	0.00183	0.51131	0.01952	0.06701	0.00103	0.01975	0.00107	426	72	419	13	418	6	395	21
WSMG-1-13	188	320	0.59	0.05540	0.00127	0.51513	0.01457	0.06745	0.00091	0.02073	0.00064	428	50	422	10	421	5	415	13
WSMG-1-14	148	221	0.67	0.05584	0.00223	0.51937	0.02298	0.06745	0.00110	0.01981	0.00134	446	86	425	15	421	7	397	27
WSMG-1-15	124	178	0.69	0.05525	0.00170	0.51052	0.01801	0.06705	0.00099	0.02059	0.00101	422	67	419	12	418	6	412	20

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表 2 红旗沟正长花岗岩主量元素(%)、微量元素和稀土元素(10^-6)分析结果

Table 2. Major elements (%), trace and REE elements (10^-6) data of the Hongqigou syenogranite

样号	WSMG-2	WSMG-3	WSMG-4	WSMG-7	WSMG-8
SiO₂	76.6	78.4	77.4	77.4	76.0
Al₂O₃	12.3	11.0	11.8	11.8	12.0
Fe₂O₃	1.39	1.09	1.18	1.21	1.61
MnO	0.01	0.02	0.01	0.01	0.02
MgO	0.20	0.11	0.12	0.16	0.22
CaO	0.29	0.79	0.50	0.27	0.51
Na₂O	3.25	2.93	3.19	3.19	3.19
K₂O	5.22	4.64	4.96	4.93	5.02
TiO₂	0.15	0.12	0.12	0.13	0.17
P₂O₅	0.02	0.01	0.01	0.02	0.02
LOI	0.66	1.01	0.80	0.66	1.00
Total	100.18	100.26	100.23	99.92	99.94
K₂O/Na₂O	1.61	1.58	1.55	1.55	1.57
Na₂O+K₂O	8.47	7.57	8.15	8.12	8.21
A/CNK	1.06	0.97	1.02	1.06	1.03
Tzr(℃)	800	782	787	798	800
Li	6.22	5.46	4.65	6.20	6.40
Be	2.54	3.62	2.29	2.69	3.15
Sc	2.25	1.91	1.95	2.18	2.51
V	2.69	3.23	2.63	3.09	3.71
Cr	19.7	19.7	16.5	13.7	13.2
Co	117.2	98.2	129.6	123.5	110.5
Ni	117	104	160	150	110
Cu	2.98	2.69	4.08	2.79	7.84
Zn	29.0	48.9	26.2	27.9	27.8
Ga	20.3	18.0	19.4	19.3	20.0
Rb	219	208	220	213	221
Sr	52.1	49.4	48.8	50.7	56.5
Y	72.4	68.5	76.8	73.7	75.8
Zr	172	150	153	166	178
Nb	8.67	8.87	6.76	8.49	9.49
Sn	4.71	4.62	4.89	4.53	6.15
Cs	3.56	3.58	3.47	3.41	3.68
Ba	219	193	207	219	237
La	55.4	53.3	54.0	69.7	52.5
Ce	112.7	94.6	109.3	84.3	109.9
Pr	13.0	11.1	12.7	9.82	12.8
Nd	48.9	42.2	48.1	37.6	48.9
Sm	9.02	8.14	8.99	7.37	9.40
Eu	0.30	0.26	0.28	0.29	0.29
Gd	8.57	7.71	8.58	7.20	9.16
Tb	1.33	1.24	1.35	1.19	1.52
Dy	7.25	6.96	7.43	6.98	8.79
Ho	1.38	1.34	1.44	1.40	1.73
Er	4.16	3.99	4.40	4.24	5.23
Tm	0.58	0.56	0.63	0.62	0.76
Yb	3.76	3.66	4.11	4.04	4.90
Lu	0.57	0.55	0.62	0.62	0.74
Hf	4.26	5.66	5.88	6.24	6.85
Ta	1.62	1.97	1.75	2.48	1.70
Pb	23.3	25.4	22.6	21.9	22.1
Th	21.7	20.3	21.7	20.3	26.1
U	4.55	4.26	3.58	4.81	4.56
10⁴×Ga/Al	3.13	3.09	3.10	3.09	3.15
Zr+Nb+Ce+Y	365.7	321.9	346.1	332.5	373.4
Nb/Ta	5.36	4.50	3.87	3.43	5.58
∑REE	266.9	235.6	261.9	235.4	266.6
LREE	239.3	209.6	233.4	209.1	233.8
HREE	27.6	26.0	28.6	26.3	32.8
LREE/HREE	8.66	8.06	8.17	7.96	7.13
Eu/Eu^*	0.10	0.10	0.09	0.12	0.09
(La/Yb)_N	10.6	10.5	9.4	12.4	7.7
(Gd/Yb)_N	1.9	1.7	1.7	1.5	1.6
注：LOI.烧失量；A/CNK=molar Al₂O₃/(CaO+Na₂O+K₂O).

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表 3 红旗沟正长花岗岩全岩Sm-Nd同位素分析结果

Table 3. Sm-Nd isotopic compositions of the Hongqigou syenogranite

点号	¹⁴⁷Sm/¹⁴⁴Nd	¹⁴³Nd/¹⁴⁴Nd	±1σ	(¹⁴³Nd/¹⁴⁴Nd)_t	ε_Nd(t)	t_DM2(Ma)
WSMG-8	0.116307	0.512305	0.000018	0.511985	-2.2	1 339
WSMG-7	0.118468	0.512299	0.000080	0.511973	-2.4	1 359
WSMG-4	0.113062	0.512280	0.000014	0.511969	-2.5	1 365
注：ε_Nd(t)值计算采用球粒陨石(CHUR)的¹⁴⁷Sm/¹⁴⁴Nd=0.1967；¹⁴³Nd/¹⁴⁴Nd=0.512638(Depaolo and Wasserburg, 1979)；t_DM2(Ma)计算采用亏损地慢(DM)的¹⁴⁷Sm/¹⁴⁴Nd=0.2136；¹⁴³Nd/¹⁴⁴Nd=0.513151(Jahn and Condie, 1995)；¹⁴⁷Sm衰变常数λ=6.54×10^-12·a^-1(Steiger and Jger, 1977).

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表 4 红旗沟正长花岗岩(WSMG-1)锆石Hf同位素分析结果

Table 4. Hf isotopic data for sample WSMG-1 from the Hongqigou syenogranite

点号	年龄(Ma)	¹⁷⁶Yb/¹⁷⁷Hf	±2σ	¹⁷⁶Lu/¹⁷⁷Hf	±2σ	¹⁷⁶Hf/¹⁷⁷Hf	±2σ	ε_Hf(t)	t_DM1(Ma)	t_DM2(Ma)	f_Lu/Hf
WSMG-1	418	0.037667	0.000759	0.001270	0.000023	0.282536	0.000030	0.5	1021	1374	-0.96
WSMG-2	420	0.044778	0.001885	0.001507	0.000056	0.282522	0.000030	0.0	1047	1408	-0.95
WSMG-3	422	0.026073	0.000356	0.000981	0.000013	0.282576	0.000025	2.1	957	1277	-0.97
WSMG-4	420	0.029585	0.000775	0.001066	0.000027	0.282441	0.000025	-2.8	1149	1583	-0.97
WSMG-5	417	0.046558	0.000689	0.001642	0.000022	0.282488	0.000024	-1.3	1100	1489	-0.95
WSMG-6	423	0.024552	0.000026	0.000912	0.000002	0.282482	0.000019	-1.2	1087	1487	-0.97
WSMG-7	421	0.027438	0.000073	0.000984	0.000004	0.282527	0.000017	0.3	1025	1386	-0.97
WSMG-8	420	0.038105	0.000543	0.001431	0.000024	0.282558	0.000019	1.3	994	1327	-0.96
WSMG-9	422	0.021057	0.000102	0.000792	0.000004	0.282493	0.000020	-0.8	1068	1460	-0.98
WSMG-10	419	0.040054	0.000337	0.001422	0.000010	0.282554	0.000022	1.1	999	1335	-0.96
WSMG-11	420	0.037694	0.000193	0.001362	0.000006	0.282541	0.000022	0.7	1015	1362	-0.96
WSMG-12	418	0.023493	0.000175	0.000862	0.000005	0.282516	0.000018	-0.1	1037	1411	-0.97
WSMG-13	421	0.028334	0.000888	0.001022	0.000031	0.282529	0.000021	0.4	1023	1383	-0.97
WSMG-14	421	0.031175	0.000322	0.001147	0.000013	0.282548	0.000021	1.0	1000	1344	-0.97
WSMG-15	418	0.028654	0.001421	0.001044	0.000040	0.282580	0.000031	2.1	952	1269	-0.97
注：f_Lu/Hf=(¹⁷⁶Lu/¹⁷⁷Hf)_S/(¹⁷⁶Lu/¹⁷⁷Hf)_CHUR-1；ε_Hf(t)=10000×{[(¹⁷⁶Hf/¹⁷⁷Hf)_S-(¹⁷⁶Lu/¹⁷⁷Hf)_S×(e^λt-1)]/[(¹⁷⁶Hf/¹⁷⁷Hf)_{CHUR, 0}-(¹⁷⁶Lu/¹⁷⁷Hf)_CHUR×(e^λt-1)]-1}；t_DM1=1/λ×ln{1+[(¹⁷⁶Hf/¹⁷⁷Hf)_S-(¹⁷⁶Hf/¹⁷⁷Hf)_DM]/[(¹⁷⁶Lu/¹⁷⁷Hf)_S-(¹⁷⁶Lu/¹⁷⁷Hf)_DM；t_DM2=t_DM(Hf)-(t_DM(Hf)-t)×[(f_CC-f_S)/(f_CC-f_DM)]；(¹⁷⁶Lu/¹⁷⁷Hf)_CHUR=0.0332，(¹⁷⁶Hf/¹⁷⁷Hf)_{CHUR, 0}=0.28272(Blichert-oft et al., 1997)，(¹⁷⁶Lu/¹⁷⁷Hf)_DM=0.0332，(¹⁷⁶Hf/¹⁷⁷Hf)_DM=0.282772(Griffin et al., 2000)，f_CC=0.015，f_DM=-0.548，λ=1.867×10^-11·a^-1(Söderlund et al., 2004).

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