Rb-Sr Isochron Age and Its Geological Significance of Baishaziling Tin Deposit in Dayishan Ore Field, Hunan Province
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摘要: 大义山矿田处于华南褶皱带南岭成矿带中段北缘，位于阳明山－大义山－上堡东西向基底断裂、攸县－宁远北东向基底断裂和郴州－邵阳北西向隐伏深断裂带的交汇部位，主要受大义山岩体控制，其中云英岩脉型锡矿为该矿田典型的成矿类型之一.对该矿田白沙子岭锡矿床云英岩脉型锡矿脉中的石英进行了流体包裹体Rb-Sr同位素测年及其地质意义的讨论.结果显示，矿脉中石英流体包裹体Rb-Sr同位素等时线年龄为160±1 Ma，属于南岭地区中生代160~150 Ma时段成矿高峰期产物；成矿与大义山岩体中侏罗世二长花岗岩具有密切的时间、空间和成因联系，为该期岩浆晚期热液成矿作用的产物；流体包裹体Rb-Sr同位素87Sr/86Sr初始比值为0.706 79±0.003 66，预示其成矿流体有幔源物质的参与，具有地壳和地幔混合流体的特征.Abstract: Dayishan ore field located in the north rim of the middle section of the Nanling metallogenic belt in South China fold zone, and at the intersection of Yangmingshan-Dayishan-Shangpu EW basement fault, Youxian-Ningyuan NE basement fault and Chenzhou-Shaoyang NW concealed deep fault, has been controlled by the Dayishan intrusive rock. The greisens-vein type tin deposit is one of the typical mineralization types in this ore field. The Rb-Sr geochronology of fluid inclusions in quartz of the ore veins is presented and its geological significance of the Baishaziling greisens-vein type tin deposit is discussed in this paper. The Rb-Sr isotopic dating of fluid inclusions of quartz is 160±1 Ma, which indicates that the tin deposit was likely formed in the peaks (160-150 Ma) of Mesozoic mineralization period of Nanling region, and the mineralization was closely related to the magmatic intrusion of the Middle Jurassic monzogranite of Dayishan intrusive rock, as a result of the post-magmatic hydrothermal mineralization. The initial 87Sr/86Sr value of the fluid inclusions is 0.706 79±0.003 66, which may indicate a mantle-derived fluid contribution to the ore-forming fluids.
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Key words:
- Rb-Sr /
- isotopes /
- quartz fluid inclusion /
- monzogranite /
- geochronology /
- mineral deposit
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图 1 大义山矿田区域位置(据陈庆等，2005)
1.侏罗系－白垩系；2.泥盆系－三叠系；3.震旦系－奥陶系；4.花岗岩体；5.深大断裂带及编号；6.级构造单元分界线；7.主要断裂及编号；8.典型内生金属矿产.主要断裂名称：(1)NE向宁远－常宁深大断裂带；(2)EW向九嶷山－大东山基底褶皱带；(3)NW向郴州－邵阳断裂带；①阳明山－大义山－上堡东西向基底断裂；②攸县－宁远北东向基底断裂；③郴州－邵阳北西向隐伏深断裂带
Fig. 1. Geological sketch map of the Dayishan ore field
图 2 湘南大义山矿田锡多金属矿产地质简图(伍光英等，2005)
D-P.泥盆系－二叠系; .震旦系－寒武系; J3ηγ.晚侏罗世二长花岗岩; J2ηγ.中侏罗世二云二长花岗岩; J2βηγ.中侏罗世黑云二长花岗岩; J1βkγ.早侏罗世黑云钾长花岗岩; 1.地质界线; 2.左行走滑断裂; 3.大型矿床; 4.中小型矿床; 5.白沙子岭矿区
Fig. 2. The geological sketch map of the tin-polymetallic deposits in the Dyishan ore field, southern Hunan Province
图 3 大义山地区白沙子岭锡矿床地质简图(据曾志方等, 2008)
1.第四系地层；2.马兰边组；3.孟公坳组；4.中侏罗世二云二长花岗岩; 5.中侏罗世黑云二长花岗岩; 6.矽卡岩; 7.取样位置及编号; 8.锡矿脉及编号; 9.断层
Fig. 3. The geological map of the Baishaziling tin deposit in the Dayishan ore field
图 4 白沙子岭锡矿床典型矿石及镜下典型矿物照片
a.石英－锡石－电气石脉型矿石; b.石英－锡石－毒砂脉型矿石; c.含矿云英岩脉; d.毒砂(Apy)、锡石(Cst)共生; e.黄铜矿(Ccp)、锡石(Cst)共生; f.黝锡矿(Sta)、闪锌矿(Sp)与黄铜矿(Ccp)共生
Fig. 4. Photos of typical ores and microscopic images of typical minerals in the Baishaziling tin deposit
图 5 白沙子岭锡矿床云英岩脉型锡矿体中石英流体包裹体Rb-Sr等时线
Fig. 5. Rb-Sr isochron of fluid inclusion in quartzes from the greisen vein orebody of the Baishaziling tin deposit
表 1 大义山岩体岩性及年龄数据
Table 1. The Lithology and chronology of Dayishan intrusive rock
时代 代号 岩性 年龄(Ma) 测试方法 数据来源 晚侏罗世 J3ηγ 中细－细(微)粒二长花岗岩 141，143，144 B 湖南地质矿产勘查局，湖南1∶5万白沙镇幅区域地质调查报告，1988；伍光英等，2005 中侏罗世 J2ηγ 细粒(少斑)二云二长花岗岩 156 B 伍光英等, 2005 J2βηγ 中粗－细(微)粒斑状黑云二长花岗岩 169，181，177 B 湖南地质矿产勘查局，湖南1∶5万白沙镇幅区域地质调查报告，1988；伍光英等, 2005 早侏罗世 J1βkγ 中－细粒斑状(含角闪石)黑云钾长花岗岩 174 Z 湖南地调院，湖南1∶5万罗家桥幅、阳嘉洲幅区域地质调查报告，2000 注：B.黑云母K-Ar法；Z.独居石U-Pb模式年龄. 
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表 2 大义山矿田白沙子岭锡矿床云英岩脉型矿体中石英流体包裹体Rb-Sr同位素组成
Table 2. Rb-Sr isotopic compositions of fluid inclusion in quartzes from the greise vein type orebody of the Baishaziling tin deposit
序号 样品编号 矿物 Rb(10-6) Sr(10-6) 87Rb/86Sr 87Sr/86Sr(2σ) t(Ma) 1 Rb-1 石英 0.412 6 0.041 7 28.75 0.775 89±0.000 04 160±1(1σ) 2 Rb-2 石英 3.647 0 0.058 2 188.10 1.126 82±0.000 04 3 Rb-3 石英 4.205 0 0.047 3 272.00 1.330 66±0.000 07 4 Rb-4 石英 1.010 0 0.043 7 67.59 0.856 17±0.000 05 5 Rb-5 石英 5.618 0 0.159 4 104.00 0.949 13±0.000 06 6 Rb-6 石英 3.988 0 0.075 3 157.90 1.058 22±0.000 10 7 Rb-7 石英 6.198 0 0.058 9 325.30 1.451 28±0.000 08 8 Rb-8 石英 1.940 0 1.760 0 3.18 0.718 72±0.000 05 9 Rb-9 石英 5.594 0 0.103 0 162.20 1.071 34±0.000 06
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表 3 湘南地区部分花岗岩体及钨锡多金属矿床成岩成矿年龄
Table 3. Rock-forming and ore-forming ages of some tungsten-tin polymetallic deposits in southern Hunan Province
矿区 岩体 成岩年龄(Ma) 成矿年龄(Ma) 测试方法 文献 大义山 大义山岩体 160±1 石英Rb-Sr等时线年龄 本文 黄沙坪 花岗斑岩 162 LA-ICPMS锆石U-Pb年龄 姚军明等, 2005 黄沙坪 花岗斑岩 153.8±4.8 辉钼矿Re-Os等时线年龄 马丽艳等，2007 黄沙坪 花岗斑岩 154.8±1.9 辉钼矿Re-Os等时线年龄 姚军明等，2005 金船塘 千里山岩体 133.4±5.9 石英Rb-Sr等时线年龄 马丽艳等，2010 金船塘 千里山岩体 141±11 符山石、石榴石Sm-Nd等时线年龄 马丽艳等，2010 金船塘 千里山岩体 164±12 辉铋矿－黄铁矿Pb-Pb等时线年龄 肖红全等，2003 金船塘 千里山岩体 158.8±6.6 辉钼矿Re-Os等时线年龄 刘晓菲等，2012 红旗岭 千里山岩体 143.1±8.7 石英Rb-Sr等时线年龄 马丽艳等，2010 红旗岭 千里山岩体 155~151 153.3±1 白云母Ar-Ar坪年龄 袁顺达等，2012 柿竹园 千里山岩体 151.1±3.5 辉钼矿Re-Os等时线年龄 李红艳等, 1996 瑶岗仙 瑶岗仙岩体 154.9±2.6 辉钼矿Re-Os等时线年龄 Peng et al., 2006 瑶岗仙 瑶岗仙岩体 153.0±1.1 金云母Ar-Ar坪年龄 Peng et al., 2006 瑶岗仙 瑶岗仙岩体 155.1±1.1 白云母Ar-Ar坪年龄 Peng et al., 2006 香花岭 香花岭岩体 151.9±3 白云母Ar-Ar等时线年龄 Yuan et al., 2007 香花岭 香花岭岩体 160.0±3.2 白云母Ar-Ar等时线年龄 Yuan et al., 2007 香花岭 香花岭岩体 160.3±3.2 白云母Ar-Ar等时线年龄 Yuan et al., 2007 大坳 九嶷山岩体 151.3±2.4 辉钼矿Re-Os等时线年龄 付建明等, 2007 骑田岭 骑田岭岩体 155.5±1.3 锆石SHRIMP U-Pb年龄 赵葵东等，2006 骑田岭 骑田岭岩体 157.1±1.2 锆石SHRIMP U-Pb年龄 赵葵东等，2006 骑田岭 角闪黑云花岗岩 157.5±0.3 黑云母Ar-Ar坪年龄 毛景文等, 2004b 骑田岭 三门锡矿 156.1±0.4 白云母Ar-Ar坪年龄 毛景文等, 2004b 骑田岭 淘洗窝锡矿 160.1±0.9 白云母Ar-Ar坪年龄 毛景文等, 2004b 白腊水
骑田岭岩体南溪单元 146±10 Rb-Sr等时线年龄 李华芹等，2006 含矿花岗斑岩体 146±5 锆石SHRIMP U-Pb年龄 李华芹等，2006 主花岗岩体 155±6 锆石SHRIMP U-Pb年龄 李华芹等，2006 矿化花岗岩 156±5 锆石SHRIMP U-Pb年龄 李华芹等，2006 矿化花岗岩 137±5 Rb-Sr等时线年龄 李华芹等，2006 矿化花岗岩 133±15 Sm-Nd等时线年龄 李华芹等，2006
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