辽东岫岩晚侏罗世荒地岩体的地球化学、年代学与Hf同位素及构造意义

薛吉祥; 刘正宏; 刘杰勋; 董晓杰; 冯帆; 连光辉

doi:10.3799/dqkx.2020.008

辽东岫岩晚侏罗世荒地岩体的地球化学、年代学与Hf同位素及构造意义

doi: 10.3799/dqkx.2020.008

吉林大学地球科学学院, 吉林长春, 130061

基金项目:

国家自然科学基金项目 41272223

国家自然科学基金项目 41340024

中国地质调查局项目 12120113098500

详细信息

作者简介:
薛吉祥(1994-), 男, 硕士研究生, 构造地质学专业

通讯作者:
刘正宏

中图分类号: P581;P597
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- 被引次数: 0
出版历程
- 收稿日期: 2019-11-02
- 刊出日期: 2020-06-15

Geochemistry, Geochronology, Hf Isotope and Tectonic Significance of Late Jurassic Huangdi Pluton in Xiuyan, Liaodong Peninsula

College of Earth Sciences, Jilin University, Changchun 130061, China

摘要

摘要: 辽东半岛中生代晚侏罗世岩浆活动较少，研究程度较低.通过对辽宁岫岩县荒地花岗岩岩体进行锆石U-Pb测年、岩石地球化学和锆石Lu-Hf同位素分析来进一步了解辽东半岛晚侏罗世的构造动力学背景，荒地花岗岩的岩浆锆石U-Pb加权平均年龄为161.1±3.6 Ma（MSWD=1.4），表明荒地岩体的形成时代为晚侏罗世，为燕山期岩浆活动的产物.该岩体含白云母等富铝矿物，地球化学数据也显示，该岩体为过铝质高钾钙碱性系列，富集K、Rb、Cs、Ba等大离子亲石元素，亏损Nb、Ti、P等高场强元素，具轻稀土元素富集，重稀土元素亏损的特征，Eu为中等负异常（δEu=0.33~0.80）.该花岗岩A/CNK平均值为1.10，CIPW标准矿物中出现刚玉分子（>1%）.由此认为该岩体为经历了高程度的结晶分异作用的S型花岗岩.荒地花岗岩CaO/Na₂O比值小于0.3，ε_Hf（t）小于0（-36.968~-23.298），表明该岩石由地壳的泥质岩熔融形成.两阶段Hf模式年龄T_DM^C=2 680~3 568 Ma，表明该岩体源岩的组成物质从地幔储库中脱离的时间为新太古代至古太古代，同时与辽东半岛侏罗纪其他花岗岩进行了比较.综上所述，该岩体形成于古太平洋板块向欧亚大陆俯冲后俯冲角度变大、向更深处俯冲的背景之下.
- 荒地岩体 /
- 华北克拉通 /
- 锆石U-Pb年龄 /
- Hf同位素 /
- S型花岗岩 /
- 地球化学
Abstract: Late Jurassic magmatic activity in the Liaodong Peninsula was less and the research degree was lower. In this paper, zircon U-Pb dating, geochemistry and zircon Lu-Hf isotope analysis were carried out to further understand the tectonic dynamics of the Liaodong Peninsula in the Late Jurassic. The U-Pb weighted mean age of magmatic zircons in the Huangdi granite is 161.1±3.6 Ma (MSWD=1.4), indicating that the formation of the Huangdi granite is the Late Jurassic, which is the product of the Yanshanian magmatism. The pluton contains muscovite and other aluminum-rich minerals geochemical data show that the pluton is the peraluminum calcium alkaline series, enriched with LILE such as K, Rb, Cs, and Ba, and depleted HFSE such as Nb, Ti, and P. With the characteristics of light rare earth element enrichment and heavy rare earth element loss, Eu is a moderate negative anomaly (δEu=0.33-0.80).The average A/CNK value of the granite is 1.10, and the corundum molecule (>1%) appears in the CIPW standard mineral. It is considered that the pluton is an S-type granite that has undergone a high degree of crystallization differentiation. The CaO/Na₂O ratio of the Huangdi granite is less than 0.3, and the ε_Hf(t) is less than 0 (-36.968 to -23.298), indicating that the rock is formed by the mudstone of the earth's crust. The single-stage Hf mode age is T_DM=1 728-2 311 Ma, the two-stage Hf mode age is T_DM^C = 2 680-3 568 Ma. It is shown that the time when the constituent materials of the source rock of the pluton were separated from the mantle reservoir was Neo-Archean to Ancient Archean.In summary, the pluton is formed in the background of the ancient Pacific plate subduction to the Eurasian continent and the subduction angle becomes larger and submerged deeper.
- Huangdi pluton /
- North China craton /
- zircon U-Pb age /
- Hf isotope /
- S-type granite /
- geochemistry

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图 1 大地构造位置图(a)和辽东半岛中生代岩浆岩分布图(b)

图a据赵国春(2009)；图b据Wu et al.(2005)

Fig. 1. Geological regional location map of study area (a) and distribution of Mesozoic intrusions in the Liaodong Peninsula(b)

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图 2 辽东半岛岫岩县荒地地区地质简图

1.第四纪；2.小岭组；3.小东沟组；4.温家沟组；5.锉草沟组；6.二长花岗岩；7.似斑状二长花岗岩；8.二长花岗岩；9.闪长岩；10.黑云母二长花岗岩；11.伟晶岩；12.辽河群；13.韧性变形界线；14.韧性剪切带；15.推测性质不明断层；16.实测性质不明断层；17.航磁解译断层；18.构造破碎带；19.角度不整合界线；20.采样点

Fig. 2. Geological sketch map of Huangdi area in Xiuyan, Liaodong Peninsula

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图 3 荒地花岗岩镜下照片

a.B3088⁃1；b.B4028⁃1；c.B6005⁃1；d.DYN⁃1；荒地花岗岩手标本照片e和f.Pl.斜长石；Qz.石英；Mi.微斜长石；Bit.黑云母；Mu.白云母

Fig. 3. Microscope photograghs for Huangdi granite rocks

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图 4 辽东半岛荒地花岗岩的SiO₂⁃K₂O图解(a)和A/CNK⁃A/NK图解(b)

图a据Peccerillo and Taylor (1976)；b据Shand(1943)

Fig. 4. Plots of SiO₂⁃K₂O (a) and A/CNK⁃A/NK (b) for Huangdi granites, Liaodong Peninsula

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图 5 球粒陨石标准化稀土元素配分曲线(a)和辽东半岛荒地花岗岩的原始地幔标准化微量元素蛛网图(b)

球粒陨石值据Boynton(1984)；原始地幔值据Sun and McDonough(1989)

Fig. 5. Chondrite⁃normalized REE patterns (a) and primitive mantle⁃normalized trace element patterns of the granite from the Huangdi pluton in Xiuyan, Liaodong Peninsula (b)

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图 6 辽东半岛荒地花岗岩部分锆石阴极发光图像

实线圆圈代表锆石U⁃Pb测试位置；虚线圆圈代表锆石Hf同位素测试位置

Fig. 6. CL images of representative zircons from Huangdi granites in Liaodong Peninsula

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图 7 辽东半岛荒地锆石U⁃Pb协和年龄图

Fig. 7. SHRIMP U⁃Pb concordia diagram of zircons of the granites from Huangdi pluton in Xiuyan, Liaodong Peninsula

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图 8 荒地花岗岩锆石的T⁃ε_Hf(t)图解

Fig. 8. T⁃ε_Hf(t) plot for the zircons of Huangdi granite

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图 9 Sr/Y⁃Y图解(a)和(La/Yb)_N⁃Yb_N图解(b)

Fig. 9. Sr/Y⁃Y (a) and (La/Yb)_N⁃Yb_N (b) diagrams of the Huangdi granite in Xiuyan, Liaodong Peninsula

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图 10 Rb⁃(Y+Nb)图解(a)、Nb⁃Y图解(b)、Rb⁃(Ta+Yb)图解(c)

syn⁃COLG为同碰撞花岗岩，VAG为火山弧花岗岩，WPG为板内花岗岩，ORG为洋中脊花岗岩；据Pearce et al. (1984)

Fig. 10. Rb⁃Y+Nb diagram(a), Nb⁃Y diagram(b), Rb⁃Ta+Yb diagram(c) of Huangdi granite in Xiuyan, Liaodong Peninsula

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表 1 荒地花岗岩的主量元素(%)和微量元素(10^-6)分析结果

Table 1. Major (%) and trace (10^-6) element concentrations of the granite rocks from Huangdi area

	DYN⁃1	B4028⁃1	B6005⁃1	B3088⁃1
SiO₂	73.6	73.9	74.6	73.7
TiO₂	0.11	0.09	0.11	0.14
Al₂O₃	14.40	14.30	13.85	14.35
Fe₂O₃	1.03	1.06	1.42	1.39
MnO	0.02	0.02	0.03	0.03
MgO	0.17	0.15	0.17	0.27
CaO	1.24	0.70	0.89	1.18
Na₂O	3.98	3.97	3.76	4.01
K₂O	4.08	4.66	4.45	3.89
P₂O₅	0.03	0.03	0.03	0.03
FeO^T	0.93	0.95	1.28	1.25
Total	98.66	98.88	99.31	98.99
K₂O/Na₂O	1.03	1.17	1.18	0.97
K₂O+Na₂O	8.06	8.63	8.21	7.90
A/CNK	1.09	1.11	1.10	1.11
A/NK	1.31	1.24	1.26	1.33
Ba	851	576	909	1350
Rb	144.0	211	209	138.5
Sr	378	206	289	495
Zr	75	65	100	134
Nb	8.1	13.4	17.4	10.1
Cr	20	30	30	40
La	26.3	26.8	45.7	46.8
Ce	48.4	51.7	85.9	86.4
Pr	4.98	5.05	8.21	7.76
Nd	16.7	17.9	27.9	26.2
Sm	2.73	3.26	4.66	4.22
Eu	0.58	0.39	0.46	0.98
Gd	2.01	2.64	3.64	2.98
Tb	0.33	0.39	0.63	0.49
Dy	1.94	2.02	3.57	2.58
Ho	0.40	0.36	0.73	0.54
Er	1.26	1.18	2.46	1.78
Tm	0.17	0.18	0.34	0.24
Yb	1.12	1.12	2.45	1.62
Lu	0.13	0.14	0.35	0.24
Y	12.3	11.8	24.8	16.8
Cs	1.00	1.10	2.31	0.75
Ta	0.7	0.9	1.7	1.0
Hf	2.0	2.2	3.4	3.5
ΣREE	107.05	113.13	187	182.83
LREE	99.69	105.1	172.83	172.36
HREE	7.36	8.03	14.17	10.47
LREE/HREE	13.54	13.09	12.20	16.46
(La/Yb)_N	15.83	16.13	12.58	19.48
δEu	0.73	0.39	0.33	0.80
Rb/Sr	0.38	1.02	0.72	0.28
Nb/Ta	11.57	14.89	10.24	10.10
CaO/Na₂O	0.31	0.18	0.24	0.29
Rb/Sr	0.38	1.02	0.72	0.28
Rb/Ba	0.17	0.37	0.23	0.10
Rb/Nb	17.78	15.75	12.01	13.71
Zr/Hf	37.5	29.5	29.4	38.3
Sr/Ba	1.51	1.31	1.29	1.63
DI	89.69	92.15	90.54	88.69
刚玉	1.26	1.53	1.29	1.47

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表 2 荒地白云母二长花岗岩的LA⁃MC⁃ICP⁃MS锆石U⁃Pb分析结果

Table 2. LA⁃MC⁃ICP⁃MS zircon U⁃Pb data of the muscovite monzogranite from Huangdi pluton in Xiuyan, Liaodong Peninsula

测点号	元素含量(×10^-6)			Th/ U	同位素比值						同位素年龄(Ma)
测点号	Pb	Th	U	Th/ U	²⁰⁷Pb/ ²⁰⁶Pb	1σ	²⁰⁷Pb/ ²³⁵U	1σ	²⁰⁶Pb/ ²³⁸U	1σ	²⁰⁷Pb/ ²⁰⁶Pb	1σ	²⁰⁷Pb/ ²³⁵U	1σ	²⁰⁶Pb/ ²³⁸U	1σ
DYN⁃1⁃1	25.7	82.9	1 026	0.08	0.050 3	0.002 4	0.170	0.007	0.024 8	0.000 5	209	109	159	6	158	3
DYN⁃1⁃2	171.8	182.1	487	0.37	0.116 8	0.002 2	4.957	0.093	0.307 5	0.003 7	1 907	33	1 812	16	1 728	18
DYN⁃1⁃3	6.9	72.4	198	0.37	0.045 8	0.009 1	0.217	0.048	0.032 8	0.002 0	191	29	200	40	208	12
DYN⁃1⁃5	26.6	100.5	1 044	0.10	0.050 5	0.001 8	0.173	0.006	0.024 9	0.000 4	220	51	162	5	159	2
DYN⁃1⁃8	87.1	52.7	254	0.21	0.135 2	0.008 8	5.800	0.372	0.309 8	0.007 3	2 166	113	1 946	56	1 740	36
DYN⁃1⁃9	57.5	163.3	2 227	0.07	0.049 8	0.001 2	0.177	0.005	0.025 8	0.000 4	187	57	165	4	164	3
DYN⁃1⁃10	3.7	81.4	130	0.62	0.053 3	0.006 8	0.169	0.022	0.023 9	0.000 9	339	294	158	19	152	6
DYN⁃1⁃11	95.7	105.1	351	0.30	0.113 9	0.002 1	3.723	0.069	0.237 2	0.003 0	1 863	33	1 576	15	1 372	16
DYN⁃1⁃14	89.5	162.5	251	0.65	0.117 0	0.002 2	4.700	0.092	0.290 9	0.003 1	1 922	35	1 767	16	1 646	15
DYN⁃1⁃18	40.3	251.4	1 470	0.17	0.051 4	0.001 9	0.182	0.007	0.025 7	0.000 3	261	85	170	6	164	2
DYN⁃1⁃19	6.7	188.5	213	0.89	0.059 4	0.010 5	0.177	0.028	0.025 4	0.001 2	583	391	166	25	162	7

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表 3 辽东荒地花岗岩的Hf同位素分析结果

Table 3. Hf isotope analysis results of Huangdi granite in Liaodong Peninsula

测点号	T(Ma)	¹⁷⁶Hf/¹⁷⁷Hf	¹⁷⁶Lu/¹⁷⁷Hf	¹⁷⁶Yb/¹⁷⁷Hf	1σ	ε_Hf(t)	T_DM^Hf(Ma)	T_DM^C(Ma)
DYN⁃1⁃01	158	0.282 018	0.000 81	0.040 30	3.0	-23.298 074 07	1 728	2 680
DYN⁃1⁃02	1 907	0.281 662	0.001 67	0.081 59	33.0	1.181 794 147	2 266	2 471
DYN⁃1⁃03	208	0.281 602	0.001 01	0.049 04	12.4	-36.968 833 13	2 311	3 568
DYN⁃1⁃04	159	0.281 807	0.000 68	0.029 45	2.4	-30.711 580 41	2 010	3 144
DYN⁃1⁃05	2 166	0.281 919	0.000 73	0.034 03	113.0	17.334 503 65	1 859	1 672
DYN⁃1⁃06	164	0.281 960	0.002 63	0.139 92	2.7	-25.411 689 43	1 898	2814
DYN⁃1⁃07	152	0.281 918	0.000 81	0.039 43	5.5	-26.957 914 33	1 866	2 904
DYN⁃1⁃08	1922	0.281 556	0.001 12	0.052 44	34.7	-1.557 603 622	2 380	2 652
DYN⁃1⁃09	162	0.281 929	0.001 78	0.086 19	7.4	-26.460 603 56	1 898	2 879

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